SYNTHESIS OF UNIFORM CUBE SHAPE CuFe2O4 NANOPARTICLES BY A HYDROTHERMAL METHOD
Nội dung chính của bài viết
Tóm tắt
In this study, CuFe2O4 nanoparticles (NPs) which features with superparamagnetic, and uniform cube shape structure was synthesized by a hydrothermal method. The prepared samples were characterized by scanning electron microscope (SEM), transmission electron microscopy (TEM), vibrating sample magnetometer (VSM), X-ray powder diffraction (XRD). The CuFe2O4 NPs were well dispersed with a mean particle size of about 50 nm. The CuFe2O4 NPs is extremely useful for support catalyst in heterogeneous catalysis applications and adsorption.
Từ khóa
Cube shape CuFe2O4, superparamagnetic, nanoparticles
Chi tiết bài viết
Tài liệu tham khảo
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10. A. Karimipour, S.A. Bagherzadeh, M. Goodarzi, A.A. Alnaqi, M. Bahiraei, M.R. Safaei, M.S. Shadloo, Synthesized CuFe2O4/SiO2 nanocomposites added to water/EG: evaluation of the thermophysical properties beside sensitivity analysis & EANN, International Journal of Heat and Mass Transfer, 2018, 127:1169-1179.
11. X. Dong, B. Ren, Z. Sun, C. Li, X. Zhang, M. Kong, S. Zheng, D.D. Dionysiou, Monodispersed CuFe2O4 nanoparticles anchored on natural kaolinite as highly efficient peroxymonosulfate catalyst for bisphenol A degradation, Appl. Catal. B: Environ., 2019, 253:206-217.
12. A. Goyal, S. Bansal, S. Singhal, Facile reduction of nitrophenols: Comparative catalytic efficiency of MFe 2 O 4 (M=Ni, Cu, Zn) nano ferrites, International Journal of Hydrogen Energy, 2014, 39:4895-4908.
13. S. Anandan, T. Selvamani, G.G. Prasad, A. Asiri, J. Wu, Magnetic and catalytic properties of inverse spinel CuFe2O4 nanoparticles, Journal of Magnetism and Magnetic Materials, 2017, 432:437-443.
13. L.-K. Wu, H. Wu, H.-B. Zhang, H.-Z. Cao, G.-Y. Hou, Y.-P. Tang, G.-Q. Zheng, Graphene oxide/CuFe2O4 foam as an efficient absorbent for arsenic removal from water, Chemical Engineering Journal, 2018, 334:1808-1819.
14. H. Jiao, G. Jiao, J. Wang, Preparation and Magnetic Properties of CuFe2O4 Nanoparticles, Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013, 43:131-134.
2. Z. Dong, X. Le, C. Dong, W. Zhang, X. Li, J. Ma, Ni@Pd core-shell nanoparticles modified fibrous silica nanospheres as highly efficient and recoverable catalyst for reduction of 4-nitrophenol and hydrodechlorination of 4-chlorophenol, Appl. Catal. B: Environ., 2015, 162:372-380.
3. C. Li, R. Wei, Y. Xu, A. Sun, L. Wei, Synthesis of hexagonal and triangular Fe3O4 nanosheets via seed-mediated solvothermal growth, Nano. Res., 2015, 7:536-543.
4. M. Crosswhite, J. Hunt, T. Southworth, K. Serniak, A. Ferrari, A.E. Stiegman, Development of magnetic nanoparticles as microwave-specific catalysts for the rapid, low-temperature synthesis of formalin solutions, ACS Catal., 2013, 3:1318-1323.
5. S. Si, C. Li, X. Wang, D. Yu, Q. Peng, Y. Li, Magnetic monodisperse Fe3O4 manoparticles, Crystal Growth & Design, 2005, 5:391-393.
6. B. Bateer, C. Tian, Y. Qu, S. Du, Y. Yang, Z. Ren, K. Pan, H. Fu, Synthesis, size and magnetic properties of controllable MnFe2O4 nanoparticles with versatile surface functionalities, Dalton Trans, 2014, 43:9885-9891.
7. I. Ibrahim, I.O. Ali, T.M. Salama, A.A. Bahgat, M.M. Mohamed, Synthesis of magnetically recyclable spinel ferrite (MFe2O4, M=Zn, Co, Mn) nanocrystals engineered by sol gel-hydrothermal technology: High catalytic performances for nitroarenes reduction, Appl. Catal. B: Environ., 2016, 181:389-402.
8. C. Dey, A. Chaudhuri, A. Ghosh, M.M. Goswami, Magnetic cube-shaped NiFe2O4 nanoparticles: An effective model catalyst for nitro compound reduction, ChemCatChem, 2017, 9:1953-1959.
9. Y. Xu, D. Sun, H. Hao, D. Gao, Y. Sun, Non-stoichiometric Co(ii), Ni(ii), Zn(ii)-ferrite nanospheres: size controllable synthesis, excellent gas-sensing and magnetic properties, RSC Adv., 2016, 6:98994-99002.
10. A. Karimipour, S.A. Bagherzadeh, M. Goodarzi, A.A. Alnaqi, M. Bahiraei, M.R. Safaei, M.S. Shadloo, Synthesized CuFe2O4/SiO2 nanocomposites added to water/EG: evaluation of the thermophysical properties beside sensitivity analysis & EANN, International Journal of Heat and Mass Transfer, 2018, 127:1169-1179.
11. X. Dong, B. Ren, Z. Sun, C. Li, X. Zhang, M. Kong, S. Zheng, D.D. Dionysiou, Monodispersed CuFe2O4 nanoparticles anchored on natural kaolinite as highly efficient peroxymonosulfate catalyst for bisphenol A degradation, Appl. Catal. B: Environ., 2019, 253:206-217.
12. A. Goyal, S. Bansal, S. Singhal, Facile reduction of nitrophenols: Comparative catalytic efficiency of MFe 2 O 4 (M=Ni, Cu, Zn) nano ferrites, International Journal of Hydrogen Energy, 2014, 39:4895-4908.
13. S. Anandan, T. Selvamani, G.G. Prasad, A. Asiri, J. Wu, Magnetic and catalytic properties of inverse spinel CuFe2O4 nanoparticles, Journal of Magnetism and Magnetic Materials, 2017, 432:437-443.
13. L.-K. Wu, H. Wu, H.-B. Zhang, H.-Z. Cao, G.-Y. Hou, Y.-P. Tang, G.-Q. Zheng, Graphene oxide/CuFe2O4 foam as an efficient absorbent for arsenic removal from water, Chemical Engineering Journal, 2018, 334:1808-1819.
14. H. Jiao, G. Jiao, J. Wang, Preparation and Magnetic Properties of CuFe2O4 Nanoparticles, Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013, 43:131-134.